Jakas A, Magnus V, Horvat S, Sandberg G
Synthesis of the Beta- D- Glucosyl Ester of [Carbonyl- C-13 ]- Indole- - Acetic Acid
Journal of Labelled Compounds & Radiopharmaceuticals: 1993 33:933-939
An efficient, operationally simple synthetic approach to 1-O-([carbonyl-C-13]-indole-3'-ylacetyl)-beta-D-glucopyranose is described. The synthesis was carried out by fusing a fully benzylated 1-O-glucosylpseudourea intermediate with [carbonyl-C-13]-indole-3-acetic acid, followed by hydrogenolytic removal of the protective groups.
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